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Molten salt synthesis of single crystal co3o4
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Molten salt synthesis of single crystal co3o4 nanorods
Date:23.02.2018, 23:23 The synthesis of the single-crystal Co3O4 nanorods by molten salt approach was reported for the first time. The products were characterized by Transmission electron microscopy (TEM X-ray diffraction (XRD High-resolution transmission electron microscopy (HRTEM ) and Selected-area electron diffraction (SAED ). CuCo2O4 and CuOCo3O4 compounds were prepared by a one-pot simple molten salt method (MSM) at 280 C to 750 C. Changes in morphology, crystal structure and electrochemical properties of CuCo2O4 as a function of preparation temperatures were investigated using X-Ray Diffraction (XRD Scanning Electron Microscopy (SEM) and BrunauerEmmettTeller absorption isotherm. Molten salt synthesis of single-crystal Co3O4 nanorods. Xingfei Ke, Jieming Cao, Mingbo Zheng, Yongping Chen, Jinsong Liu, Guangbin Ji. Materials Letters 2007 61 (18). CuCo2O4 and CuOCo3O4 compounds were prepared by a one-pot simple molten salt method (MSM) at 280 C to 750 C. Changes in morphology, crystal structure and electrochemical properties of CuCo2O4 as a function of preparation temperatures were investigated using X-Ray Diffraction (XRD Scanning Electron). At a current rate of 60 mA g1 and in the voltage range of V vs. Li, CuCo2O4 composite prepared at 510 C shows a high and stable capacity of 680 (quenched) and 740 (slow cooling) mAh g1 at the end of the 40th cycle.
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